Week 5 - Bottles, Samples, Testing, Storage
It has been a few weeks now since I started this thread and the practical component of this project, I don't think I have ever struggled so hard to remember (from my BSc days) basic concepts of chemistry and indeed measurement of fluids in my whole life.
Prior to commencing the practical component I had spent a good 6 to 7 months reading on perfume forums, searching the web, reading 'ancient manuscripts'
ala Toto's Africa in searches and reading so obscure, just to glean a line or two that would assist me to understand scents, their chemistry and how composition effects the final scent of a perfume come aftershave.
Chemistry is a fascinating, beautiful and truly wondrous area of the sciences - the laws and behaviour of compounds and the complexity of their 'behaviour' in dynamic conditions is flawless. I say this quite openly admitting I am a novice, there is an almost infinite amount I still have yet to learn.
Bottled, Rested, Decanted and Tested
Time-scales being what they are, and the non-real time nature of my posts and updates here leads me to this conclusion posts of sorts, a majority of the solutions have been resting and 'marrying' at 6% strength for 2 to 3 weeks now in 500ml dark amber bottles, kept in a cool dark place and agitated for 1 to 2 min every day. They are now looking, smelling and performing as an aftershave should.
Suffice to say I have been using them all daily, making notes on their effects on the face, longevity, feel, etc as well as a subjective test can. My dear wife too has been recruited to the process, yes I have subjected her to wearing a variety of men's aftershaves as I have 2 or 3 work colleagues
prior to inflicting them on P&C members who will receive the testers.
500ml Amber Boston bottles clearly labelled with Name, strength, and date make ideal storage for mixed solutions, keep them in a cool dark place and ensure you shake them every day for a minute or two. Pictured at the front in the 5ml amber bottles with drippers and 10gm tubs of post-shave balm to match the scents.
Here we see my trusty 500ml brown Boston bottles with 5ml labelled 'dripper' bottles ready to be sent to the testers. Also visible are 10gm plastic screw tubs containing the matching post-shave balm.
I have become fairly familiar with these fellows over the previous weeks, agitating them for 1 to 2 min daily, every day. The daily agitation is a must to ensure the solution is even, stable and to ensure the oils are distributed. Further to this point, the scents are smelled and compared day after day and notes are made as the scent and overall accords matures.
Here we see 5ml bottles with 'drippers' and drip proof/tamper proof caps. Also in evidence my
artistic prowess in regards to design, using scissors to cut a straight line and labelling!
Decanting to Sample bottles
1ml or 3ml Pipettes
5ml or larger bottles to hold the aftershave
Labels for the 5ml bottles -
Pre written with the name of your aftershave
I pour a quantity from the 500ml bottles into a clear 250ml beaker after shaking the 500ml bottle well. I then use a pipette to measure out 5ml and decant it into the smaller bottles and
seal them immediately to prevent spillage - not that I personally of course, would spill a 5ml bottle of splash on the dining table and endure the wrath of my wife or anything like that
Australian Private Reserve - The Scents
I have been working on around 12 to 15 scents, of which 6 of them are ready for testing in both aftershave and after shave balm. I will be sending these out to the testers this week. I am bloody nervous about how they will be received especially with the discerning, learned olfactory skills of the average P&C'er.
Australian Private Reserve – Essential Oils & Absolutes
Most essential oils I have used are certified organic by ACO or USDA and I have included the country of origin so there can be no confusion. Where an Essential Oil or Absolute is
not organic I have noted it with (NO). All EO’s and Absolutes have been sourced from large, long trading, reputable outlets. If I have made any labelling errors in this regard below they are inadvertent.
I have listed the main base, heart and top essential oils/absolutes. Obviously I have excluded some in the interests of keeping my hard earned scents to myself. Some accords here have 3 or 4 additional EO’s, there are no Fragrance Oils (when used) I have omitted.
Where I have used fragrance oils in every single instance it is clearly noted.
The Splash Ingredients
Denatured Alcohol, Witch Hazel, De mineralized Water, Poly Sorbate 20, Glycerine, Essential Oils, Fragrance Oils.
The Balm Ingredients
I am using a commercial base containing approved ingredients that is prepared by an accredited facility to Australian Standards pertaining to skin and face care products.
Ingredients: Purified Water, Vegetable Glycerine, Sunflower Oil, Essential Oils/Fragrance Oils, Cetearyl Alcohol, Capric/Caprylic Triglyceride, Jojoba Oil, Almond Sweet Oil, Shea Butter, Macadamia Oil, Phenoxyethanol, Natural Vitamin E, Ceteareth 20, Stearic Acid, Caprylyl Glycol, Carbomer, Dimethicone, Butylene Glycol, Soya Bean Oil, Sodium Hydroxide, Aloe Vera Leaf Juice Powder, Hydrolyzed Marine Collagen, Ethylhexylglycerine
The Scents - Aftershave and Post Shave Balm
PC – Un côtelette de porc – Pork Chop
This is a traditional vetiver based on a discontinued Vetiver by Creed. I don’t for a second think that I have achieved anything even close to Creed’s masterpiece. Vetivers are traditionally darker, woody scents that are autumnal or wintery in nature. They are deep, earthy, damp scents by their very nature.
Composition: Haitian Vetiver, French Oakmoss Absolute, Virginian Cedar Wood, Italian Bergamot, French Lavender, Australian Sweet Orange (NO), French Ginger
GL - les généraux du grand livre – The Generals Ledger
In the modern vocabulary of perfumery, this is a bright Fougère. A traditional Fougère has strong notes of grasses, ferns, damp earth with a slight, top note to brighten it up.
Modern Fougère varieties are generally more floral or, in this case ‘brighter’ – they have multiple notes to lighten them up, make them slightly floral and more welcoming. Another keeper, I am very pleased with this scent (I like the smell personally) and I particularly like the name and in effect tribute to the man himself, all round good guy with an epic razor collection and an equally epic
number of spreadsheets.
Composition: French Oakmoss Absolute, Haitian Vetiver, Venezuelan Tonka, French Lavender, Nutmeg, Cinnamon Bark, Egyptian Geranium, Italian Bergamot, Rose Maroc.
AC –choix Alfredus - Alfredus Choice
This is a scent that I made for a friend who happens to be part of the ‘Euro ‘A’ list limited edition shave kit set’, chemist extraordinaire and another all-round good guy. I asked him to name some scents he liked, he did so and thus it was named.
Best described as a traditional Fougère although one that is woody with subdued citrus notes from the White Grapefruit and Bergamot. As this is Alfredus choice, and as yet he has not tried it, the formula may change if he advises me he does not like it, or wants emphasis on certain notes .
Composition: Ambergris, Venezuelan Tonka, French Oakmoss Absolute, Indian Mysore Sandalwood, French Ginger, Virginian Cedarwood, Nutmeg, French Lavender, French Violet, White Grapefruit, Italian Bergamot, Basil.
SV – Sandalwood, Lime, Verbena
This came about as I was dissatisfied with the ‘L’Occitane
Verveine’ EDT that I paid $70 for. The problem with citrus EO’s and Verbena in particular is that scent doesn’t last.
Citrus top notes – Lemon, Lime and Verbena particularly are notoriously short lived.I set to making one that would last a little longer, after 15 or 20 formulas I hit upon one that I feel works. It’s nice, but simple – I will keep a bottle kicking around as I like the Verbena scents in summer.
This accord uses Essential Oils and Verbena Fragrance Oil. The next batch I do will Verbena EO that is quite expensive, but is a fragrance I really like in the hot humid months.
Composition: Australian Sandalwood, Lime, Spanish Lemon, Fragrance Oil
CS – Coconut Sandalwood
The first of the 'Mystic' companions, this one is for the limited edition Coconut Sandalwood. I have worked on the scent slightly and added essential oils alongside the fragrance oil that is used in the original soap.
This accord uses Essential Oils and Coconut Fragrance Oil.
Composition: Australian Sandalwood, Indian Mysore Sandalwood, Rosewood Oil (NO), Fragrance Oil.
WG – White Tea & Ginger
The second of the Mystic companions, again I spent some time with the scent of the original and made a few slight alterations to the Fragrance oil base adding one or two EO’s for longevity and roundness of the tea.
This accord uses Fragrance oil and Essential Oils
Composition: French Ginger, Venezuelan Tonka, Fragrance Oil.
I have made a few more scents to compliment the Mystic range as they are soaps I enjoy so much however these are not at the testing stage yet but will be soon. If anyone has a request for a scent based on a Mystic Water soap, please don't hesitate to drop me a PM - If I have the soap I will look into it for you.
SA – Suitably Attired Australian
Imagine a suitable attired gentlemen taking a leisurely walk surrounded by Green eucalyptus trees that remind him of tweed. He chances upon an Irish traveller who makes the Stirling suggestion that they take tea together.
This is another ‘interpretation’ of Creed’s Green Irish Tweed that uses the same Fragrance oil that Stirling and Mystic use in their GIT interpretations.
I have added EO’s for longevity and to liven up the heart and tops as the Fragrance Oil itself is fairly short lived and rather synthetic. It was fun to dabble, I quite like the scent but I am more interested in pure EO formulations and making something new and interesting. This is a one off.
This accord uses Essential Oils and Fragrance oil.
Composition: Ambergris, Indian Mysore Sandalwood, French Violet, Spanish Lemon, Rosemary, Australian Sweet Orange, Fragrance Oil.
Conclusion
That is it for this week, as I mentioned I will be sending out the testers and balms this week so people can tell me what they think, I am quite happy with some and incredibly happy with others. I will revisit this thread in a short time or in response to questions or such forth. I will also recap issues or steps in the process that I no doubt have forgotten to mention. I spent most of last night to around 3.30am bottling things up, mixing balm and scents, packaging, printing, decanting and so forth.
As always, questions, corrections, criticisms, advice or comments are always welcome. It's been another thoroughly enjoyable week mucking around in the kitchen, learning and smelling the whole time.